Course: Laboratory of Analytical Instrumental Methods

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Course title Laboratory of Analytical Instrumental Methods
Course code KALCH/C024
Organizational form of instruction Lesson
Level of course Bachelor
Year of study 3
Semester Winter
Number of ECTS credits 4
Language of instruction Czech
Status of course Compulsory
Form of instruction Face-to-face
Work placements This is not an internship
Recommended optional programme components None
Lecturer(s)
  • Cífková Eva, Ing. Ph.D.
  • Husáková Lenka, Ing. Ph.D.
  • Česlová Lenka, doc. Ing. Ph.D.
  • Adam Martin, doc. Ing. Ph.D.
  • Metelka Radovan, Ing. Ph.D.
  • Česla Petr, doc. Ing. Ph.D.
  • Eisner Aleš, Ing. Ph.D.
  • Bartoš Martin, Ing. CSc.
  • Ventura Karel, prof. Ing. CSc.
  • Červenka Libor, doc. Ing. Ph.D.
  • Mikysek Tomáš, Ing. Ph.D.
  • Hájek Tomáš, Ing. Ph.D.
  • Bajerová Petra, doc. Ing. Ph.D.
Course content
Spectrophotometric analysis of multicomponent samples. Automatic potentiometric titration of sample pretreated using ion-exchanger. Polarography/voltammetry - qualitative and quantitative analysis of metal ions. Molecular fluorescence analysis. Photometric microtitration. Alkalimetric titration with potentiometric and conductometric indication. Nephelometry. Coulometric titration with biamperometric indication. Spectrophotometric determination of nickel after extraction. Polarimetry. Flame photometry and atomic absorption spectrometry. Direct potentiometry with fluoride ion-selective electrode. Determination of chlorine in organic compound. Thin layer chromatography. Liquid chromatography - determination of phthalates in spirits.

Learning activities and teaching methods
Laboratory work
Learning outcomes
The aim of the course is to get basic experiences and practice the work with instrumental analytical methods.
Students after graduation of the subject "Laboratory of analytical instrumental methods" together with the subject C023 "Analytical instrumental methods" are competent to execute the simpler procedures in analytical laboratories equipped with the basic accessories
Prerequisites
unspecified
KALCH/C020
----- or -----
KALCH/C020P

Assessment methods and criteria
Written examination, Student performance assessment

Current check of study - written test, oral checking Student preparation, results of analyses, protocol - 70 % of grade Final examination (written and oral) - 30 %
Recommended literature
  • Vytřas K. a kol. Laboratorní cvičení z analytické chemie, část II: Instrumentální analýza (skripta). Pardubice, 1996.


Study plans that include the course
Faculty Study plan (Version) Branch of study Category Recommended year of study Recommended semester
Faculty of Chemical Technology Chemistry and Technical Chemistry (2015) Engineering chemistry and chemistry of silicates 3 Winter
Faculty of Chemical Technology Chemistry and Technical Chemistry (2014) Engineering chemistry and chemistry of silicates 3 Winter
Faculty of Chemical Technology Evaluation and Analysis of Foodstuffs (2015) Food industry and food industry chemistry 3 Winter
Faculty of Chemical Technology Evaluation and Analysis of Foodstuffs (2013) Food industry and food industry chemistry 3 Winter
Faculty of Chemical Technology Evaluation and Analysis of Foodstuffs (2016) Food industry and food industry chemistry 3 Winter
Faculty of Chemical Technology Chemistry and Technical Chemistry (2013) Engineering chemistry and chemistry of silicates 3 Winter
Faculty of Chemical Technology Evaluation and Analysis of Foodstuffs (2014) Food industry and food industry chemistry 3 Winter
Faculty of Chemical Technology Chemistry and Technical Chemistry (2016) Engineering chemistry and chemistry of silicates 3 Winter