Course: Analytical Chemistry I

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Course title Analytical Chemistry I
Course code KALCH/C618
Organizational form of instruction Lecture + Seminary
Level of course Bachelor
Year of study not specified
Semester Winter
Number of ECTS credits 5
Language of instruction Czech
Status of course Compulsory
Form of instruction Face-to-face
Work placements This is not an internship
Recommended optional programme components None
Lecturer(s)
  • Ventura Karel, prof. Ing. CSc.
  • Husáková Lenka, Ing. Ph.D.
  • Eisner Aleš, Ing. Ph.D.
  • Bartoš Martin, Ing. CSc.
  • Česlová Lenka, doc. Ing. Ph.D.
Course content
Introduction; Theoretical fundamentals of analytical chemistry; Chemical equilibriums in solutions; Expression of target compound content in solutions; Processing of analytical results Principles of qualitative analysis of inorganic compounds; Isolation and identification of selected ions Sample pretreatment - inorganic and organic samples, sampling, decomposition, pre concentration; Application for the environmental analysis and for analysis of working environment Principles of quantitative analysis of inorganic compounds Protolytic reactions, definitions of constants, pH, analytical application of protolytic reactions Acid-basic titrations, titration curves and their evaluation The modes of titration stop indication, examples of determinations; Titrations in non-water environment Complexing reactions, stability constants, effect of side reactions, shielding Chelatometric titrations, indicators, examples of applications including the selected mixtures determination Red-ox reactions, standard and formal potential, effect of side reactions; Principles of most important oxidimetric and reductometric volumetric methods The course of red-ox titration curve, indication, typical examples of application Precipitation reactions, solubility and solubility product, solubility affecting, precipitate properties, precipitate creation and condition selections for precipitation Examples of determinations, principles of precipitation titrations, indication, titration curves; Fundamentals of gravimetric analysis

Learning activities and teaching methods
Monologic (reading, lecture, briefing)
  • unspecified - 1 hour per semester
Learning outcomes
The aim of this course is to supply information to students about fundamentals of chemical analysis, i.e. to introduce them the basic principles of qualitative and quantitative analyses of compounds.
Students after graduation of this course are able to orientate oneself in the field of qualitative and mainly quantitative analytical methods, is introduced with the principles of individual volumetric and gravimetric methods including the sample pre-treatment methods.
Prerequisites
High school knowledge of analytical chemistry
KOANCH/C002
----- or -----
KOANCH/C222 and KALCH/C619

Assessment methods and criteria
Oral examination, Written examination, Student performance assessment

The examination consists of written part followed by the oral examination. During the semester the gained knowledge of students from lectures and seminar practices are checked up by two written tests which results are the part of the total classification. Current check of study - 2 written tests - 30 % of grade, written part of examination - 10 %, oral examination - 60 %.
Recommended literature
  • Bartoš, M., Šrámková, J., Staněk, V., Denver, F., Kalous, J. Analytická chemie I, 2004, Univerzita Pardubice..
  • Bartoš, M., Švancara, I., Šrámková, J. Laboratorní cvičení z analytické chemie I., 2004, Univerzita Pardubice..
  • Garaj, J., Bustin, D., Hladký, Z. Analytická chémia, 1987, ALFA Bratislava.
  • Gary, D. Christian. Analytical Chemistry, 1994, New York, John Wiley & Sons. New York, 1994.
  • Holzbecher , Z., Churáček, J. a kol. Analytická chemie, 1987, SNTL Praha.
  • Okáč, A. Analytická chemie kvalitativní, 1966, Academia Praha..
  • Skoog, D.A., West,D.M., Holler, J.F. Fundamentals of analytical chemistry, 1992, Saunders College Publishing.. 1992.
  • Vláčil, F. a kol. Příklady z chemické a instrumentální analýzy, 1978, 1983, SNTL Praha,; 1991, Informatorium Praha..


Study plans that include the course
Faculty Study plan (Version) Branch of study Category Recommended year of study Recommended semester
Faculty of Chemical Technology Clinical Biology and Chemistry (2015) Special and interdisciplinary fields 2 Winter
Faculty of Chemical Technology Clinical Biology and Chemistry (2014) Special and interdisciplinary fields 2 Winter
Faculty of Chemical Technology Clinical Biology and Chemistry (2016) Special and interdisciplinary fields 2 Winter
Faculty of Chemical Technology Laboratory Assistant (2014) Health service 2 Winter
Faculty of Chemical Technology Clinical Biology and Chemistry (2013) Special and interdisciplinary fields 2 Winter
Faculty of Chemical Technology Laboratory Assistant (2013) Health service 2 Winter