Course: Laboratory of Specialization II

« Back
Course title Laboratory of Specialization II
Course code KANT/C152
Organizational form of instruction Lesson
Level of course Master
Year of study 2
Semester Winter
Number of ECTS credits 9
Language of instruction Czech
Status of course Compulsory
Form of instruction Face-to-face
Work placements This is not an internship
Recommended optional programme components None
Lecturer(s)
  • Bělina Petr, Ing. Ph.D.
  • Dohnalová Žaneta, Ing. Ph.D.
  • Šulcová Petra, prof. Ing. Ph.D.
  • Svoboda Ladislav, doc. Ing. CSc.
  • Honcová Pavla, doc. Ing. Ph.D.
Course content
Work with literature, processing of bibliographic search of given theme. The theme solving by recommended methods and processes, in particular: Agricultural chemistry and inorganic analysis: Granulation of powder materials by fluid and rotary granulator. Testing of fertilizers by Czech Technical Standards Determination of sorptive capacity of materials by batch and column way. Measuring of speed dissolving of materials by static and dynamic method. Measuring of surface potential of dispersed particles. Coulometry, conductometry and potentiometry. Ion chromatography. UV-VIS photometry. Atomic Absorption Spectrometry. Complexometric, acidobazic, precipitating and redox titrations. Thermodynamics and calorimetry: Diferential scanning calorimetry. Izoperibolic reaction calorimetry. Calorimetry with thermal flow Determination of reaction heat of chemical reactions and phase transformations. Determination of solubility of compounds and its influence on temperature and ionic strength. Measuring of sorptive and heat properties of materials Calorimetric methods used in synthesis of inorganic salts. Inorganic pigments: Use of suspension method in synthesis of inorganic pigments. High temperature methods of preparation of inorganic pigments. Evaluation of effect of milling on application properties of pigments. Utilization of methods of thermal analysis in synthesis of inorganic pigments. Determination of anticorrosive efficiency of inorganic pigments. Determination of technological-application properties of inorganic pigments and powder materials. Measuring of colour properties of pigments and colour protective coatings. Determination of rheological properties of liquids. Measuring of particle size distribution Thermal analysis Public presentation of results in lecture.

Learning activities and teaching methods
Demonstration, Laboratory work
Learning outcomes
The aim of the subject is to complex familiarize the students with methods of synthesis and characterization of inorganic pigments, fertilizers and utilization of calorimetric methods for studying of material properties.
Passing the subject brings to students the ability to independently solve the theme of semestral work. They are competent to decide about choice of method appropriate for obtaining of information about studied materials. They are also able to elaborate the bibliographic search of given theme. The students are able to preset adjusted results at the professional level.
Prerequisites
Knowledge of course: Laboratory of synthesis and characterization of materials.
KANT/C070

Assessment methods and criteria
Home assignment evaluation, Student performance assessment

The way of passing the subject is by form of classified credit. Students solve the chosen theme of semestral work and obtained results present in public lecture. The resultant classification takes into account appraisal of an individual performance by supervisor, the quality of text processing and presentation of results of semestral work in the lecture.
Recommended literature
  • SÁDOVSKÁ G. A KOL. Návody k úlohám Laboratoře oboru I. Univerzita Pardubice, 2001.
  • Šolc Z., Trojan M. Speciální anorganické pigmenty I.. VŠCHT Pardubice, 1987.
  • Šulcová P., Beneš L. Experimentální metody v anorganické technologii. Univerzita Pardubice, 2002.


Study plans that include the course
Faculty Study plan (Version) Branch of study Category Recommended year of study Recommended semester
Faculty of Chemical Technology Inorganic Technology (2013) Engineering chemistry and chemistry of silicates 2 Winter
Faculty of Chemical Technology Inorganic Technology (2015) Engineering chemistry and chemistry of silicates 2 Winter
Faculty of Chemical Technology Inorganic Technology (2016) Engineering chemistry and chemistry of silicates 2 Winter